dc.contributor.author | Deniz, N. Gulsah | |
dc.contributor.author | Ibis, Cemil | |
dc.date.accessioned | 2021-03-06T13:01:56Z | |
dc.date.available | 2021-03-06T13:01:56Z | |
dc.date.issued | 2007 | |
dc.identifier.citation | Ibis C., Deniz N. G. , "The novel N, S-substituted nitro dienes from the reactions of some mono (alkylthio)-substituted 2-nitrodienes with piperazine and thiomorpholine and a structural study", INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, cilt.46, ss.674-680, 2007 | |
dc.identifier.issn | 0376-4699 | |
dc.identifier.other | vv_1032021 | |
dc.identifier.other | av_f6c0556e-893b-4ea1-8022-256fbe334cc4 | |
dc.identifier.uri | http://hdl.handle.net/20.500.12627/161647 | |
dc.description.abstract | Thiosubstituted nitrodien compounds 1a-f are obtained from 2-nitropentachlorobutadiene and some alifatic thiols. Compounds 1a-f have reacted with thiomorpholine 2 and yielded 3a-f in CH2Cl2. The compounds 5a-f have been obtained by the reactions of 1a-f with N-(diphenylmethyl)piperazine 4 in CH2Cl2. 2-Nitro-3,4,4-trichloro-1-(ethylthio)-1-[4-(1-diphenylmethyl)-piperazin-1-yl]-1,3-butadiene 5a is synthesized and its crystal structure is determined. The compound 5a crystallizes in the orthorhombic crystal system (space group P2(1)2(1)2(1)) with the unit cell parameters a = 9.4240(2) angstrom, b = 14.4007(2) angstrom, c = 18.1891(2) angstrom, alpha, beta, gamma = 90 degrees, V = 2468.48(7) angstrom(3), Z = 4. The structure has been solved by direct methods (SIR92) and refined to the residual index R-1 = 0.078. | |
dc.language.iso | eng | |
dc.subject | Biyokimya | |
dc.subject | Biyoinorganik Kimya | |
dc.subject | Temel Bilimler | |
dc.subject | Temel Bilimler (SCI) | |
dc.subject | Kimya | |
dc.subject | KİMYA, ORGANİK | |
dc.title | The novel N, S-substituted nitro dienes from the reactions of some mono (alkylthio)-substituted 2-nitrodienes with piperazine and thiomorpholine and a structural study | |
dc.type | Makale | |
dc.relation.journal | INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | |
dc.contributor.department | , , | |
dc.identifier.volume | 46 | |
dc.identifier.issue | 4 | |
dc.identifier.startpage | 674 | |
dc.identifier.endpage | 680 | |
dc.contributor.firstauthorID | 182264 | |