dc.contributor.author | ANILANMERT, BERİL | |
dc.contributor.author | Cengiz, Salih | |
dc.contributor.author | Mavis, Murat Emrah | |
dc.contributor.author | Gursu, Gokce Goksu | |
dc.contributor.author | ŞENER, HARUN | |
dc.date.accessioned | 2022-07-04T16:01:59Z | |
dc.date.available | 2022-07-04T16:01:59Z | |
dc.date.issued | 2022 | |
dc.identifier.citation | ŞENER H., ANILANMERT B., Mavis M. E. , Gursu G. G. , Cengiz S., "LC-MS/MS monitoring for explosives residues and OGSR with diverse ionization temperatures in soil & hands: 30 minutes for extraction plus elution", ACTA CHROMATOGRAPHICA, cilt.34, sa.3, ss.304-314, 2022 | |
dc.identifier.issn | 1233-2356 | |
dc.identifier.other | av_cf6bbfd5-4ab7-4e85-b689-53d181c09980 | |
dc.identifier.other | vv_1032021 | |
dc.identifier.uri | http://hdl.handle.net/20.500.12627/184775 | |
dc.identifier.uri | https://doi.org/10.1556/1326.2021.00930 | |
dc.description.abstract | A fast LC-APCI-MS/MS screening/confirmation method was developed and validated for trace analyses of 18 analytes which are explosives and organic gun shot residues including the challenging ones with diverse ionization conditions, in soil and on hands. (+) and (-) ionization modes were used after a single-step, low-volume solvent extraction procedure developed using methanol. Tape-lifting, stub, alcohol wipes, cotton bud were compared for collecting the residues from hands of a shooter. Tapelifting and stub gave the highest recoveries and tape-lifting was chosen. Gradient elution system using ammonium chloride:methanol was developed. Whole procedure lasted approximately 30 min, was validated in both matrices, applied to real samples as post-blast residues, smokeless powder and the hands of a shooter, after shooting. Most of the recoveries were >80% and since all the precisions were <15%, quantitation was possible for all. Limit of Detection (LOD) and Limit of Quantification (LOQ) values were: 0.2 54.1 and 0.3 190.0 ngg(-1) in soil, and 0.2 132.3 and 1.1 355.0 ngg(-1) in tape-lift. | |
dc.language.iso | eng | |
dc.subject | General Chemistry | |
dc.subject | Physical Sciences | |
dc.subject | Analytical Chemistry | |
dc.subject | Chemistry (miscellaneous) | |
dc.subject | Filtration and Separation | |
dc.subject | Temel Bilimler | |
dc.subject | Analitik Kimya | |
dc.subject | Temel Bilimler (SCI) | |
dc.subject | Kimya | |
dc.subject | KİMYA, ANALİTİK | |
dc.title | LC-MS/MS monitoring for explosives residues and OGSR with diverse ionization temperatures in soil & hands: 30 minutes for extraction plus elution | |
dc.type | Makale | |
dc.relation.journal | ACTA CHROMATOGRAPHICA | |
dc.contributor.department | Kütahya Sağlık Bilimleri Üniversitesi , Mühendislik Ve Doğa Bilimleri Fakültesi , Adli Bilimler Bölümü | |
dc.identifier.volume | 34 | |
dc.identifier.issue | 3 | |
dc.identifier.startpage | 304 | |
dc.identifier.endpage | 314 | |
dc.contributor.firstauthorID | 3434088 | |